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Beilstein J. Org. Chem. 2012, 8, 1213–1218, doi:10.3762/bjoc.8.135
Graphical Abstract
Figure 1: Four-fold PEEK-reactors with increasing chamber depths from left to right and different techniques ...
Scheme 1: Synthesis of carbazole (2) by photolysis.
Scheme 2: Synthesis of arylazides 2 by solid-phase synthesis.
Figure 2: Photolysis results in batch setup (flask) with a xenon lamp (400 W, λ > 345 nm).
Figure 3: Carbazole synthesis in miniaturized photoreactors Type II (PEEK and Teflon), flow control, P = 0.92...
Figure 4: Carbazole synthesis in miniaturized photoreactors Type II (PEEK and Teflon), power control, flow 26...
Figure 5: Test setup with continuously operating, miniaturized photoreactor.
Figure 6: The miniaturized photoreactor (PEEK) during photolysis.